Registered: 07/08/04
Posts: 1681
Loc: Down in Fraggle Rock
Is there a test I can do to positively identify boron nitride, or white graphite? Ideally, this would be a simple test that I could do in my kitchen...
Registered: 07/08/04
Posts: 1681
Loc: Down in Fraggle Rock
Sorry, guys. I was asked to take a look at a white powdery substance from overseas, and make a recommendation. Under a microscope, it looks like glass marbles, and it's used as a dry lubricant in a printing operation. I think it's boron nitride, but am totally unsure and was looking for some basic chemistry or analytical processes that would prove or disprove my hypothesis....
Registered: 07/08/04
Posts: 1681
Loc: Down in Fraggle Rock
FYI, wikipedia lists some of its properties: Insoluble in water, and with a melting point of 2700C. I'm no expert, but I think that's about as hot as the sun.... I tried the water solubility experiment, and also to try to dissolve it in a 30% phosphoric acid solution, which should eat just about anything that's reactive with acid. Both yielded zero results.
Edited by CJS (10/07/0806:25 PM) Edit Reason: celsius or fahrenheit?
Registered: 11/21/03
Posts: 7674
Loc: Kennewick, WA
Originally Posted By: CJS
Sorry, guys. I was asked to take a look at a white powdery substance from overseas, and make a recommendation.
CJS, sorry to hijack the topic but I couldn't resist. The last time I was asked to look at a white powdery substance from overseas I was a cop, we were making a major bust and my recommendations went something like..."You have the right to remain silent....(you know the rest) .
Now back to your regularly scheduled serious topic. Sorry.
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Registered: 02/07/03
Posts: 6403
Did some searching, cool stuff! The stuff you're talking about is 'hexagonal Boron Nitride', (h-BN) and there's also 'cubic Boron Nitride (C-BN), aka Cubic Zirconia...both seem to be nearly indestructible!
Got an acetylene torch setup? Since hBN melts at 2700°C (one website says 3000°), and an acetylene torch burns at 3200° to 3500°C, you would just barely be able to melt it. I would think that pretty much any other white powder would just vaporize(?)
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Registered: 08/06/05
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i've got no experience identifying white powdery overseas stuff and it seems you don't either (and that's not necessarily a bad thing). so i was wondering why you were asked to identify the stuff.
Edited by BToran (10/08/0807:02 AM)
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Registered: 11/21/03
Posts: 7674
Loc: Kennewick, WA
Originally Posted By: BToran
i've got no experience identifying white powdery overseas stuff and it seems you don't either (and that's not necessarily a bad thing). so i was wondering why you were asked to identify the stuff.
I was in on the bust and had the test kits in my brief case. Turned out to be very high grade cocaine. Not the kind of quantity you read about in the newspaper, but it was uncut.
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Registered: 01/14/04
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Loc: Massachusetts
Originally Posted By: CJS
Yes, I do have a torch. I'll give that a shot, and we'll see what happens.
Coming from a Chemical Engineering background, sticking a torch to any unknown is not what i'd call a proper scientific approach. If that powdery material happened to be something like Magnesium, you'd have an issue on your hands pretty quick. Not to mention flaming a powder can be explosive or result in oxidation of said substance which could result in toxic gas release. Is there a college around with a chem department??
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Registered: 01/14/03
Posts: 4288
Loc: Kansas City, MO
Originally Posted By: GoFirstClass
Originally Posted By: CJS
Sorry, guys. I was asked to take a look at a white powdery substance from overseas, and make a recommendation.
CJS, sorry to hijack the topic but I couldn't resist. The last time I was asked to look at a white powdery substance from overseas I was a cop, we were making a major bust and my recommendations went something like..."You have the right to remain silent....(you know the rest) .
Now back to your regularly scheduled serious topic. Sorry.
"Really Officer, it's not coke, it's Boron Nitride!"
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Admiral
Registered: 02/07/03
Posts: 6403
To test the stuff with a torch, you'd only need a very teensy tiny bit. Like, draw a dot with a pencil---a pile that big is oodles to test to see if it'll melt or vaporize.
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Registered: 07/08/04
Posts: 1681
Loc: Down in Fraggle Rock
Well, it melted.
Bruce, I work for a consulting firm that reverse-engineers products, mostly foods. Sometimes we get a referral from outside the food industry. A client asked us to review an existing product to see if it would be feasible to offer something competitive at a lower price. I just have to tell him what I think it is, and he does the rest.
Bruce, I work for a consulting firm that reverse-engineers products, mostly foods. Sometimes we get a referral from outside the food industry. A client asked us to review an existing product to see if it would be feasible to offer something competitive at a lower price.
Sure its not malamine?
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